Aldrichimica Acta, Vol. 42, No. 2, 2008.

The latest Aldrichimica Acta is out- No. 2 of volume 41. This publication was started by a friend, teaching colleague, mentor, and former boss who spent some of his best years working for Alfred Bader. He eventually retired as a VP of something or other at Aldrich. A truly great guy. For a while, the task of catalog publishing was his job. He bought paper by the rail car. Their job was to increase the size of the collection by 15 % per year.

He also invented the coffee pot kugelrohr system that Aldrich sold for a long time. It has now morphed out of recognition. But he showed me the prototype motor assembly. It consisted of a reciprocating air motor built for automotive windshield wipers wired onto some pegboard. The air motor used either air pressure or vacuum and had a metal tube that connected the vac line from one side of the motor axially to the other.  The reciprocating motor got around the need for a sealed vacuum bearing. To one side of the reciprocating tube was connected a vacuum line via flexible rubber hose, and to the other via hose and barbed connector, a series of bulb tubes and pot. 

The coffee pot came from a West Bend coffee pot plant down the road in Milwaukee. Aldrich bought the reject pots and paid a guy to refit them for kugelrohr duty in his garage. It was a very successful product. When I went to grad school we had a Buchi kugelrohr for bulb-to-bulb short path distillation. But I still remember with some fondness having to sit at the bench twiddling the Aldrich kugelrohr by hand while feeding dry ice onto the receiver. Sometimes we would drip dichloromethane in the receiver and let the evaporative cooling do the trick. We’d use the air motor for lengthy distillations.

4 thoughts on “Aldrichimica Acta, Vol. 42, No. 2, 2008.

  1. Jordan

    Between you and “Milkshake” we have lots of good stories to read. It’s easy to forget these days what Aldrich was like “back in the day” — improvised glassware assembled in garages, miscellaneous compounds bought from academic labs, etc.

    Bader is a hero at Queens University in Kingston, Ontario, his alma mater (Kingston is about 2 1/2 hrs east of Toronto, halfway between Toronto and Montreal). He is a major benefactor and donated a castle in England (IIRC) for the school’s use.

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  2. Rich Apodaca

    The coffee pot Kugelrohr was pure genius. It had a cooking thermometer stuck into the side and a teflon sleve to keep the bulb from rubbing against the pot’s side. You’d control the temperature by setting a Variac. I’ll never forget the ‘psss-psss’ sound it made as compressed air pushed through the motor.

    Aldrich must have been able to sell it for at least 200x what it cost to build. All of its competitors were even more expensive, and most were more complicated as well.

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